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[16] [23] Detecting a small increase in risk would require extremely large populations and prolonged follow-up periods
Samples were then transferred into vials and directly injected into the GCMS system (7890A gas chromatograph coupled with a triple quadrupole 7000C, Agilent Technologies) equipped with a high-sensitivity electronic impact source operating in positive mode
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This method involved pre-column derivatization of carnitines with 1-aminoanthracene in a phosphate buffer, using 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride as a catalyst
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